Bruker
BrukerOxford 400The main NMR Facility in RM 394-5 Essex Hall has 3 spectrometers that are intended for the use of researchers in the Department. There are a recently upgraded 500 MHz instrument with solution and solids NMR capabilities and two 300 MHz solution spectrometers. An additional spectrometer is located in RM B82 Essex Hall and is dedicated for use by undergraduate student lab courses when they are in session and for researchers otherwise.
Main NMR Facility
CORe Building Rm 120
Updated Summer 2012
Bruker AVANCEIII 500 MHz- Solution and Solid State
- MASII controller unit for Solid samples
- GraspII Gradient Controller
- BLAH300 1H/19F linear amplifier
- BLAX500 Broadband linear amplifier
- QNP Switching Module for 19F, 1H output selection
- HPPR/2 preamplfier stack
- TOPSPIN3.2
Solution Probes
- BBFO ( Broad Band Fluorine Optimized)
- TBI 1H, 13C, BB
- LC 1H 13C Flow Probe
Solid State Probes
- 1.3 mm MAS Probe
- 4mm MAS Probe
- Static Low Gamma Probe
DPX300 US
- Location: Rm 394-5 Essex Hall
- The "US" in the model number represents ultra shield.
- List of NMR Experiments:
1D 13C Setup and 1D 1H Setup Instructions
VT Experiments
Blue sign up book
This is a two channel instrument equipped with:
- Narrow bore magnet ((Bruker SpectroSpin, 300MHz, 7.0 Tesla)
- Broadband Observe probe tunable for X between 31P and 109Ag
- z-gradient generator for pfg experiments
- ATM (automatic tune and match) probe head
- BVT3200 variable temperature unit for VT work
- CASE automatic sample changer accessory
- WINXP workstation, Topspin2.1
This instrument can be used for routine single pulse, gradient COSY, NOESY, EXSY, HMQC, HSQC, HMBC experiments.
- Location: Rm 394-5, Essex Hall
- Yelllow sign up book
- List of NMR Experiments:
1D 13C Setup and 1D 1H Setup Instructions
VT Experiments
This is a two channel instrument equipped with:
- Narrow bore magnet (Bruker SpectroSpin, 300MHz, 7.0 Tesla)
- Broadband Observe probe tunable for X between 31P and109Ag
- WINXP workstation, TOPSPIN1.3
Location: Rm B82 Essex Hall
This instrument is used by the undergraduate laboratory course and by researchers outside of lab times.
This is a two channel instrument equipped with:
- Narrow bore magnet (Bruker SpectroSpin, 7.0 Tesla)
- QNP probe switchable for X from 13C, 31P and 19F
- WINXP workstation, TOPSPIN 1.3
- used for undergraduate student labs
400 MHz Solid State NMR System (Schurko Lab)
Oxford 400MHz Wide Bore Magnet
Bruker HD Console, MAS capabilities, assortment of probes
Bruker EPR System